Reaction of Hydrazoic Acid with Ethyl 2, 2-Dialkylacetoacetates
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چکیده
منابع مشابه
Synthesis of MgO Nanoparticales and Identificationof Their Destructive Reaction Products by 2-Chloroethyl Ethyl Sulfide
Nanocrystalline magnesium oxides were prepared by sol–gel method and were characterized by X-ray diffraction, N2-BET, SEM and infrared spectroscopy techniques. The results confirmed the formation of Nano- MgO materials with crystallite size in range of 5-20 nm and surface areas of 336-556m2/g. The product has been tested as destructive adsorbent for the decontamination of (2-chloroethyl) et...
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متن کاملEthyl 2-acetylhydrazono-2-phenylacetate
The title compound, C(12)H(14)N(2)O(3), was synthesized as an inter-mediate for the synthesis of metamitron. The benzene ring forms dihedral angles of 86.3 (2) and 10.0 (3)° with the ethyl group and the acetyl-imino plane, respectively. The crystal structure involves inter-molecular C-H⋯O and N-H⋯O hydrogen bonds.
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The methine C atom of the triphenyl-methyl group in the title compound, C(28)H(23)IO(2)S, is slightly flattened out [ΣC(phen-yl)-C-C(phen-yl) = 335.6 (5)°]. The -C-O-C-C-S- chain connecting the triphenyl-methyl group and the aromatic ring adopts an extended zigzag conformation, these five atoms lying on an approximate plane (r.m.s. deviation = 0.120 Å).
متن کاملThe Vibration Spectra of Hydrazoic Acid, Methyl Azide, and Methyl Isocyanate The Thermodynamic Functions of Hydrazoic Acid
The vibration spectra of hydrazoic acid, methyl azide, and methyl isocyanate have been investigated in the spectral region between 2 and 20~. Correlation of the spectra of these structurally similar molecules has made possible the determination of all the fundamental frequencies of hydrazoic acid and all but the methyl torsion frequency in the methyl compounds. From these fundamental frequencie...
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ژورنال
عنوان ژورنال: Chemical and Pharmaceutical Bulletin
سال: 1958
ISSN: 0009-2363,1347-5223
DOI: 10.1248/cpb.6.729